Synthesis of Hirsutene

C15H24
Principal investigator | Paul A. Wender |
---|---|
Publication year | 1982 |
Synthesis type | Total |
Number of steps | 8 (linear) |
References |
Part 1 of 1
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hν
Cyclohexane

LiAlH4
Et2O
22-23% (2 steps)

Camphorsulfonic acid
PhH
RT, 71%

PhSH
100 °C, 78%


H2
CH2Cl2
"No yield reported. Several cycling were need to fully convert this product."

NaIO4
MeOH
86%

P(OMe)3
PhH
170 °C, 60%
