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Named reactions

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Search synthesis

Sylvone

Chemical structure of Sylvone
C23H28O8
Author Tomislav Rovis
Publication year 2008
Synthesis type Total synthesis
Number of steps 6 (linear)
Reference

Browse hundreds of other total syntheses.

Part 1 of 1
Chemical structure
+
Chemical structure
TsOH
Dean-Stark
PhH
Reflux, 85%
Chemical structure + Chemical structure
Pd(OAc)2, Et3NBn+ Cl-, i-Pr2NEt
DMF
80 °C, 45%

See the Heck Coupling
Chemical structure
TMSOTf
EtCN
-78 °C

Selectivity : 90:10 R/S
Chemical structure
NaBH4
MeOH

Selectivity : 90:10 R/S
Chemical structure
OsO4, NMO
Acetone, t-BuOH, H2O

Selectivity : 90:10 R/S
See the Upjohn Dihydroxylation
Chemical structure
NaIO4
THF, H2O
85% (4 steps)
Chemical structure

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