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Named reactions

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Search synthesis

Corannulene

Chemical structure of Corannulene
C20H10
Author Jay S. Siegel
Publication year 1999
Synthesis type Total synthesis
Number of steps 10 (linear)
References

Browse hundreds of other total syntheses.

Part 1 of 1
Chemical structure
(CH2O)n, HCl
AcOH, H2O
50 °C, 24 h, 62%

See the Blanc Halomethylation
Chemical structure
KCN
Acetone, H2O
Reflux, 12 h, 99%
Chemical structure
H2SO4
AcOH, H2O
Reflux, 6 h, 90%
Chemical structure
SOCl2
CHCl3
Reflux, 60 min
Chemical structure
AlCl3
PhNO2
RT, 2 d, 82% (2 steps)

See the Friedel-Crafts Acylation
Chemical structure
SeO2
Dioxane , H2O
60 °C, 2 d, 91%
Chemical structure + Chemical structure
KOH
MeOH
RT, 30 min, 85%

See the Aldol Addition
See the Aldol Condensation
Chemical structure + Chemical structure
Ac2O
125 °C, 30 h, 74%

See the Diels-Alder Reaction
Chemical structure
NBS, Bz2O2
CCl4
Reflux, 15 h, 100%

See the Wohl-Ziegler Reaction
Chemical structure
Zn-Cu, TiCl4
DME
Reflux, 2 d, 80%
Chemical structure

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