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Named reactions

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Methoxatin

"Dedicated with respect and affection to professor R. A. Raphael on the occasion of his sixty-fifth birthday."

Chemical structure of Methoxatin
C14H6N2O8
Author Charles W. Rees
Publication year 1983
Synthesis type Total synthesis
Number of steps 11 (linear)
References

Browse hundreds of other total syntheses.

Part 1 of 1
Chemical structure
BnBr, K2CO3
Acetone
Reflux, 24 h, 92 %
Chemical structure
LiAlH4
THF
0 °C, 2 h, 83 %
Chemical structure
BaMnO4
CHCl3
Reflux, 60 min, 100 %
Chemical structure
+
Chemical structure
NaOMe
MeOH, THF
-10 to 2 °C, 18 h, 90 %

See the Aldol Condensation
Chemical structure
Xylene(s)
Reflux, 4 h, 82 %

See the Hemetsberger Indole Synthesis
Chemical structure
HCl
MeOH
Reflux, 6 h, 58 %
Chemical structure
+
Chemical structure
HCl
CH2Cl2
RT, 24 h, 95 %

See the Doebner-Miller Reaction
Chemical structure
H2, Pd/C
1 atm
MeOH
RT, 20 h, 89 %
Chemical structure
Reagent structure
MeOH, CHCl3
RT, 16 h, 93 %
Chemical structure
HC(OMe)3, TsOH
MeOH
Reflux, 3 h
Chemical structure
K2CO3, HCl
H2O
85 °C, 4 h, 79 % (2 steps)
Chemical structure

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