Synthesis of Centrohexaindane

Structure of Centrohexaindane

C41H24

Principal investigatorDietmar Kuck
Publication year1995
Synthesis typeTotal
Number of steps 6 (linear)
References
Part 1 of 1
intermediate structure + intermediate structure
TsOH
PhH
Reflux, 2 h, 90%
intermediate structure
LiAlH4
THF
Reflux, 3 h, 92%
intermediate structure
H3PO4
Xylene(s)
Reflux, 5-8 h, 33%
intermediate structure
Br2
CCl4
Reflux, , 96%
intermediate structure
AlBr3
PhH
RT, 3 d, 40%
intermediate structure
Pd/C
500 °C, 90 min, <5%
intermediate structure