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Named reactions

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Search synthesis

Thiarubrine A

Chemical structure of Thiarubrine_A
C13H8S2
Author Masato Koreeda
Publication year 1994
Synthesis type Total synthesis
Number of steps 8 (linear)
Reference

Browse hundreds of other total syntheses.

Part 1 of 1
Chemical structure
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Chemical structure
KOH
DMF
RT, 3.5 h, 87%
Chemical structure
Dess-Martin Periodinane
CH2Cl2
RT, 30 min, 91%

See the Dess-Martin Oxidation
Chemical structure
CBr4, Ph3P
CH2Cl2
0 °C, 50 min, 89%

See the Corey-Fuchs Reaction
Chemical structure
  1. n-BuLi
  2. MeI
  3. BF3.OEt2, DMF
THF
-78 °C to RT, 9.5 h

See the Corey-Fuchs Reaction
Chemical structure
CBr4, Ph3P
CH2Cl2
0 °C, 50 min, 34% (2 steps)

See the Corey-Fuchs Reaction
Chemical structure
n-BuLi
THF
-78 °C to RT, 9.5 h, 54%

See the Corey-Fuchs Reaction
Chemical structure
VinylBr, Pd(PPh3)4, CuI, Et3N
PhMe
RT, 4.5 h, 41%

See the Sonogashira Coupling
Chemical structure
n-Bu4N+ F-, I2
3Å MS
THF
RT, 3 h, 53%
Chemical structure

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