Synthesis of Hirsutene
C15H24
| Principal investigator | Alan C. Weedon |
|---|---|
| Publication year | 1987 |
| Synthesis type | Formal |
| Number of steps | 7 (linear) |
| References |
Part 1 of 1
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Imidazole,
TBSCl
CH2Cl2, DMF
0 °C to RT, 2 h, 89%
+
+
n-Bu4N+ F-
THF
RT, 12 h, 52%
H2,
PtO2
1 atm
MeOH
RT, 10 h
Remaining...
70% (1 step)
"Tetrahedron Lett. 1976, 17, 195."