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Named reactions

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Cubane

Chemical structure of Cubane
C8H8
Author John Tsanaktsidis
Publication year 1997
Synthesis type Total synthesis
Number of steps 10 (linear)
References

Browse hundreds of other total syntheses.

Part 1 of 1
Chemical structure
(CH2OH)2, Dowex 50WX8 ®
Dean-Stark
PhH
Reflux, 30 h, 90%
Chemical structure
Br2
Dioxane
RT, 2 d
Chemical structure
NaOH
MeOH
Reflux, 2 h, 60% (2 steps)

See the Diels-Alder Reaction
Chemical structure
H2SO4
RT, 30.5 h, 92%
Chemical structure
HCl
MeOH, H2O
RT
Chemical structure
NaOH
H2O
Reflux, 5 h

See the Favorskii Rearrangement
Chemical structure
Dowex 50WX8 ®
MeOH
Reflux, 24 h, 47% (3 steps)

See the Fischer Esterification
Chemical structure
NaOH
MeOH, H2O
Reflux, 4 h, 99%
Chemical structure
SOCl2
Reflux, 2 h
Chemical structure
Reagent structure
t-BuSH, DMAP
THF
Reflux, 90 min, 77% (2 steps)

See the Barton Decarboxylation
Chemical structure

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