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Taiwaniaquinol B

Chemical structure of Taiwaniaquinol_B

Author	Dirk Trauner
Publication year	2006
Synthesis type	Total synthesis
Number of steps	6 (linear)
Reference	J. Am. Chem. Soc. 2006, 128, 11022.

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Part 1 of 1

Chemical structure

NBS

DMF
RT, 42 h, 98 %

Chemical structure

+

Chemical structure

n-BuLi

Et₂O
-25 °C to RT, 105 min, 89 %

Chemical structure

Dess-Martin Periodinane

CH₂Cl₂, Pyr
RT, 5 min, 90 %

See the Dess-Martin Oxidation

Chemical structure

TMSOTf

MeNO₂
105 °C, 65 min, 70 %

See the Nazarov Cyclization Reaction

Chemical structure

BCl₃

CH₂Cl₂
0 °C, 15 min, 90 %

Chemical structure

(NH₄)₂Ce(NO₃)₆, Na₂S₂O₄

MeCN, CH₂Cl₂, H₂O
0 °C, 4 h, 51 %

Chemical structure

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