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Search synthesis

LY311727

Chemical structure of LY311727
C22H27N2O5P
Author Michael J. Martinelli
Publication year 1996
Synthesis type Total synthesis
Number of steps 8 (linear)
Reference

Browse hundreds of other total syntheses.

Part 1 of 1
Chemical structure
+
Chemical structure
MeNO2
RT, 2 d, 52%

See the Nenitzescu Indole Synthesis
Chemical structure
MeI, NaOH, n-Bu4N+ Br-
H2O
Reflux, 30 min, 80%
Chemical structure
LiAlH4
THF
0 °C, 4 h, 78%
Chemical structure
TMSCN, BF3.OEt2
CH2Cl2
0 °C, 60 min, 83%
Chemical structure
KOH
t-BuOH
Reflux, 60 min, 85%
Chemical structure
BBr3
CH2Cl2
0 °C, 2 h, 80%
Chemical structure + Chemical structure
KOH, K2CO3, n-Bu4N+ Br-
DMF
RT, 16 h, 89%
Chemical structure
TMSI
CH2Cl2
RT, 90 min, 92%
Chemical structure

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