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Named reactions

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Search synthesis

Cyclophellitol

Chemical structure of Cyclophellitol
C7H12O5
Author Ken-Ichi Sato
Publication year 1994
Synthesis type Total synthesis
Number of steps 13 (linear)
Reference

Browse hundreds of other total syntheses.

Part 1 of 1
Chemical structure
i-Pr2NLi
THF, CH2Cl2
-78 °C, 82%
Chemical structure
NaBH4
DMSO
80 °C, 82%
Chemical structure
Ac2O
Pyr
RT, 100%
Chemical structure
NBS, BaCO3
CCl4
Reflux

See the Hanessian-Hullar Reaction
Chemical structure
NaI
Acetone
Reflux

See the Finkelstein Reaction
Chemical structure
DBU
4 Å MS
DMSO
80 °C, 60 min, 56% (3 steps)
Chemical structure
HgCl2
Acetone, H2O
Reflux, 60 min

See the Petasis-Ferrier Rearrangement
Chemical structure
MsCl, Et3N
CH2Cl2
0 °C, 86% (2 steps)
Chemical structure
NaBH4, CeCl3.7H2O
EtOH, CH2Cl2
-78 °C, 67%

See the Luche Reduction
Chemical structure
TBSCl, Imidazole
DMF
40 °C, 94%
Chemical structure
KOH
EtOH
RT, 20 min, 80%
Chemical structure
mCPBA
DCE
40 °C, 24 h, 84%

See the Prilezhaev Reaction
Chemical structure
AcOH
H2O
RT, 60 min, 100%
Chemical structure

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