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Named reactions

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Search synthesis

Ampelopsin F

Chemical structure of Ampelopsin_F
C28H22O6
Author Scott A. Snyder
Publication year 2007
Synthesis type Total synthesis
Number of steps 12 (linear)
Reference

Browse hundreds of other total syntheses.

Part 1 of 1
Chemical structure
NaBH4
MeOH
0 °C, 30 min
Chemical structure
PBr3, Pyr
Et2O
40 °C, 3 h, 93 % (2 steps)
Chemical structure
NBS
CH2Cl2
0 °C, 60 min, 95 %
Chemical structure
HP(O)(OEt)2, TMS2NK
THF
0 °C to RT, 12.5 h, 91 %
Chemical structure
+
Chemical structure
KOt-Bu
THF
-78 °C to RT, 13.5 h, 98 %

See the Horner-Wadsworth-Emmons Reaction
Chemical structure
+
Chemical structure
n-BuLi
THF
-78 °C to RT, 5.5 h, 71 %
Chemical structure
+
Chemical structure
TsOH
CH2Cl2
-50 °C to RT, 17.5 h, 65 %

See the Prins Reaction
Chemical structure
mCPBA, NaHCO3
CH2Cl2
0 °C to RT, 3 h, 78 %
Chemical structure
KOH
t-BuOH, CCl4, H2O
80 °C, 12 h, 52 %

See the Ramberg-Bäcklund Reaction
Chemical structure
Br2
CH2Cl2
-78 °C to RT, 4 h, 53 %

See the Friedel-Crafts Alkylation
Chemical structure
TMS3SiH, AIBN
PhMe
100 °C, 8 h, 89 %
Chemical structure
BBr3
CH2Cl2
0 °C to RT, 19 h, 90 %
Chemical structure

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