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Ampelopsin F
| Author | Scott A. Snyder |
|---|---|
| Publication year | 2007 |
| Synthesis type | Total synthesis |
| Number of steps | 12 (linear) |
| Reference |
Browse hundreds of other total syntheses.
Part 1 of 1
NaBH4
MeOH
0 °C, 30 min
0 °C, 30 min
PBr3, Pyr
Et2O
40 °C, 3 h, 93 % (2 steps)
40 °C, 3 h, 93 % (2 steps)
NBS
CH2Cl2
0 °C, 60 min, 95 %
0 °C, 60 min, 95 %
HP(O)(OEt)2, TMS2NK
THF
0 °C to RT, 12.5 h, 91 %
0 °C to RT, 12.5 h, 91 %
+ 
+ 
n-BuLi
THF
-78 °C to RT, 5.5 h, 71 %
-78 °C to RT, 5.5 h, 71 %
+ 
mCPBA, NaHCO3
CH2Cl2
0 °C to RT, 3 h, 78 %
0 °C to RT, 3 h, 78 %
TMS3SiH, AIBN
PhMe
100 °C, 8 h, 89 %
100 °C, 8 h, 89 %
BBr3
CH2Cl2
0 °C to RT, 19 h, 90 %
0 °C to RT, 19 h, 90 %
