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Named reactions

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Search synthesis

Pallidol

Chemical structure of Pallidol
C28H22O6
Author Scott A. Snyder
Publication year 2007
Synthesis type Total synthesis
Number of steps 12 (linear)
Reference

Browse hundreds of other total syntheses.

Part 1 of 1
Chemical structure
NaBH4
MeOH
0 °C, 30 min
Chemical structure
PBr3, Pyr
Et2O
40 °C, 3 h, 93% (2 steps)
Chemical structure
NBS
CH2Cl2
0 °C, 60 min, 95%
Chemical structure
HP(O)(OEt)2, TMS2NK
THF
0 °C to RT, 12.5 h, 91%
Chemical structure + Chemical structure
KOt-Bu
THF
-78 °C to RT, 13.5 h, 98%

See the Horner-Wadsworth-Emmons Reaction
Chemical structure + Chemical structure
n-BuLi
THF
-78 °C to RT, 4.5 h, 71%
Chemical structure + Chemical structure
TsOH
CH2Cl2
-30 °C to RT, 17 h, 65%

See the Prins Reaction
Chemical structure
mCPBA, NaHCO3
CH2Cl2
0 °C to RT, 3 h, 70%
Chemical structure
KOH
t-BuOH, CCl4, H2O
80 °C, 12 h, 55%

See the Ramberg-Bäcklund Reaction
Chemical structure
Br2
CH2Cl2
-78 °C to RT, 4 h, 81%

See the Friedel-Crafts Alkylation
Chemical structure
H2, Pd/C
1 atm
MeOH
RT, 24 h, 76%
Chemical structure
BBr3
CH2Cl2
0 °C to RT, 24 h, 83%
Chemical structure

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