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Named reactions

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Search synthesis

Longifolene

Chemical structure of Longifolene
C15H24
Author Arthur G. Schultz
Publication year 1985
Synthesis type Formal synthesis
Number of steps 16 (linear)
Reference

Browse hundreds of other total syntheses.

Part 1 of 1
Chemical structure
+
Chemical structure
K
NH3, THF, t-BuOH
-78 °C, 98%

See the Birch Reduction
Chemical structure
HCl
MeOH
Chemical structure
ClCO2Me, NaHCO3
Chemical structure
HCl, HC(OMe)3
MeOH
Reflux
Chemical structure
NaOMe
MeOH
75% (4 steps)
Chemical structure
NBS
MeOH
95%
Chemical structure
DBU
PhMe
Reflux, 85%
Chemical structure
TsOH
Acetone
Reflux, 86%
Chemical structure + Chemical structure
Chemical structure
Xylene(s)
Reflux, 40% (2 steps)
Chemical structure
H2, Pd/C
EtOH
RT, 92%
Chemical structure
KOH
MeOH, H2O
RT, 85%
Chemical structure
PhMe
Reflux, 86%
Chemical structure

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Remaining...
75% (3 steps)

See : J. Am. Chem. Soc. 1978, 100, 2583.
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