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Named reactions

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Ammosamide B

Chemical structure of Ammosamide_B
C12H10ClN5O2
Author Mark Cushman
Publication year 2010
Synthesis type Total synthesis
Number of steps 9 (linear)
Reference

Browse hundreds of other total syntheses.

Part 1 of 1
Chemical structure
NH3
Ethylene Glycol
140 °C, 3 h, 88%
Chemical structure
Boc2O, DMAP
DMF
RT, 12 h, 80%
Chemical structure
CF3CO2H
CH2Cl2
0 °C, 4 h, 90%
Chemical structure
H2, Pd/C
2 atm
EtOAc
RT, 12 h, 85%
Chemical structure + Chemical structure
TsOH, Cu(OAc)2
CHCl3
Reflux, 8.5 h, 50%

See the Doebner-Miller Reaction
Chemical structure
NCS
DMF
60 °C, 30 min, 75%
Chemical structure
CF3CO2H
CH2Cl2
RT, 6 h, 65%
Chemical structure
MeI, NaH
DMF
RT, 30 min, 70%
Chemical structure
NH3
H2O, THF
RT, 24 h, 80%
Chemical structure

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