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Named reactions

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Search synthesis

Ammosamide B

Chemical structure of Ammosamide_B
C12H10ClN5O2
Author William Fenical
Publication year 2010
Synthesis type Total synthesis
Number of steps 17 (linear)
Reference

Browse hundreds of other total syntheses.

Part 1 of 1
Chemical structure
HNO3, H2SO4
H2O
0 °C, 90 min, 58%
Chemical structure
t-BuNH2
Dioxane
100 °C, ON, 87%
Chemical structure
MeI, NaH
DMF
0 °C to RT, 45 min
Chemical structure
CF3CO2H
CH2Cl2
RT, 30 min, 92% (2 steps)
Chemical structure + Chemical structure
CH2Cl2
3.5 h, 86%

See the Wittig Reaction
Chemical structure
CF3CO2H
100 °C, ON
Chemical structure
HNO3, H2SO4
H2O
RT, ON
Chemical structure
POCl3
100 °C, ON, 85% (3 steps)
Chemical structure
HI
MeCN, H2O
RT, ON
Chemical structure
(CF3CO)2O
Pyr
0 °C, 4 min, 74% (2 steps)
Chemical structure
CuCN
Pyr
80 °C, 2 h

See the Rosenmund-von Braun Reaction
Chemical structure
H2SO4
MeOH
60 °C, ON
Chemical structure
KOH
MeOH
50 °C, 4 h
Chemical structure
H2SO4
MeOH
60 °C, 60 min

See the Fischer Esterification
Chemical structure
SOCl2
RT, 45 min
Chemical structure
(CF3CO)2O
Pyr
RT, 3 h, 8% (6 steps)
Chemical structure
Mg3N2
MeOH
0 to 80 °C, ON, 100%
Chemical structure

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