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Named reactions

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Search synthesis

Twistane

Chemical structure of Twistane
C10H16
Author Pierre Deslongchamps
Publication year 1967
Synthesis type Total synthesis
Number of steps 7 (linear)
Reference

Browse hundreds of other total syntheses.

Part 1 of 1
Chemical structure
HC(OEt)3, TsOH
EtOH
-20 to 0 °C, 60 min, 65 %
Chemical structure
Li
NH3, THF, EtOH
-33 °C, 60 min, 99 %
Chemical structure
MsCl, Pyr
CH2Cl2
-10 °C, 24 h
Chemical structure
(CO2H)2
Et2O, H2O
RT, 2 h, 59 % (2 steps)
Chemical structure
NaH
Dioxane
Reflux, 5 h, 85 %
Chemical structure
(CH2SH)2, BF3.OEt2
AcOH
RT, 16 h, 100 %
Chemical structure
Ni (Raney)
EtOH
Reflux, 5 h, 70 %
Chemical structure

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